Identification of different oxygen species in oxide nanostructures with 17O solid-state NMR spectroscopy

Meng Wang; Xin-Ping Wu; Sujuan Zheng; Li Zhao; Lei Li; Li Shen; Yuxian Gao; Nianhua Xue; Xuefeng Guo; Weixin Huang; Zhehong Gan; Frédéric Blanc; Zhiwu Yu; Xiaokang Ke; Weiping Ding; Xue-Qing Gong; Clare P. Grey; Luming Peng

doi:10.1126/sciadv.1400133

Research ArticleSURFACE CHEMISTRY

Identification of different oxygen species in oxide nanostructures with ¹⁷O solid-state NMR spectroscopy

Meng Wang¹,
Xin-Ping Wu²,
Sujuan Zheng¹,
Li Zhao¹,
Lei Li¹,
Li Shen¹,
Yuxian Gao³,
Nianhua Xue¹,
Xuefeng Guo¹,
Weixin Huang³,
Zhehong Gan⁴,
Frédéric Blanc⁵,⁶,
Zhiwu Yu⁷,
Xiaokang Ke¹,
Weiping Ding¹,
Xue-Qing Gong²,*,
Clare P. Grey⁵,⁸,* and
Luming Peng¹,*

¹Key Laboratory of Mesoscopic Chemistry of Ministry of Education, School of Chemistry and Chemical Engineering, Nanjing University, Nanjing 210093, China.
²Key Laboratory for Advanced Materials, Centre for Computational Chemistry and Research Institute of Industrial Catalysis, East China University of Science and Technology, 130 Meilong Road, Shanghai 200237, China.
³Department of Chemical Physics, University of Science and Technology of China, Hefei 230026, China.
⁴National High Magnetic Field Laboratory, 1800 East Paul Dirac Drive, Tallahassee, FL 32310–3706, USA.
⁵Department of Chemistry, University of Cambridge, Lensfield Road, Cambridge CB2 1EW, UK.
⁶Department of Chemistry and Stephenson Institute for Renewable Energy, University of Liverpool, Crown Street, Liverpool L69 7ZD, UK.
⁷High Magnetic Field Laboratory, Chinese Academy of Sciences, Hefei 230031, China.
⁸Department of Chemistry, Stony Brook University, Stony Brook, NY 11974–3400, USA.

↵*Corresponding authors. E-mail: luming{at}nju.edu.cn (L.P.); xgong{at}ecust.edu.cn (X.-Q.G.); cpg27{at}cam.ac.uk (C.P.G.)

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Science Advances 20 Feb 2015:
Vol. 1, no. 1, e1400133
DOI: 10.1126/sciadv.1400133

Meng Wang

1Key Laboratory of Mesoscopic Chemistry of Ministry of Education, School of Chemistry and Chemical Engineering, Nanjing University, Nanjing 210093, China.

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Xin-Ping Wu

2Key Laboratory for Advanced Materials, Centre for Computational Chemistry and Research Institute of Industrial Catalysis, East China University of Science and Technology, 130 Meilong Road, Shanghai 200237, China.

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Sujuan Zheng

1Key Laboratory of Mesoscopic Chemistry of Ministry of Education, School of Chemistry and Chemical Engineering, Nanjing University, Nanjing 210093, China.

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Li Zhao

1Key Laboratory of Mesoscopic Chemistry of Ministry of Education, School of Chemistry and Chemical Engineering, Nanjing University, Nanjing 210093, China.

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Lei Li

1Key Laboratory of Mesoscopic Chemistry of Ministry of Education, School of Chemistry and Chemical Engineering, Nanjing University, Nanjing 210093, China.

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Li Shen

1Key Laboratory of Mesoscopic Chemistry of Ministry of Education, School of Chemistry and Chemical Engineering, Nanjing University, Nanjing 210093, China.

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Yuxian Gao

3Department of Chemical Physics, University of Science and Technology of China, Hefei 230026, China.

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Nianhua Xue

1Key Laboratory of Mesoscopic Chemistry of Ministry of Education, School of Chemistry and Chemical Engineering, Nanjing University, Nanjing 210093, China.

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Xuefeng Guo

1Key Laboratory of Mesoscopic Chemistry of Ministry of Education, School of Chemistry and Chemical Engineering, Nanjing University, Nanjing 210093, China.

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Weixin Huang

3Department of Chemical Physics, University of Science and Technology of China, Hefei 230026, China.

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Zhehong Gan

4National High Magnetic Field Laboratory, 1800 East Paul Dirac Drive, Tallahassee, FL 32310–3706, USA.

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Frédéric Blanc

5Department of Chemistry, University of Cambridge, Lensfield Road, Cambridge CB2 1EW, UK.

6Department of Chemistry and Stephenson Institute for Renewable Energy, University of Liverpool, Crown Street, Liverpool L69 7ZD, UK.

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Zhiwu Yu

7High Magnetic Field Laboratory, Chinese Academy of Sciences, Hefei 230031, China.

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Xiaokang Ke

1Key Laboratory of Mesoscopic Chemistry of Ministry of Education, School of Chemistry and Chemical Engineering, Nanjing University, Nanjing 210093, China.

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Weiping Ding

1Key Laboratory of Mesoscopic Chemistry of Ministry of Education, School of Chemistry and Chemical Engineering, Nanjing University, Nanjing 210093, China.

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Xue-Qing Gong

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For correspondence: luming@nju.edu.cn xgong@ecust.edu.cn cpg27@cam.ac.uk

Clare P. Grey

5Department of Chemistry, University of Cambridge, Lensfield Road, Cambridge CB2 1EW, UK.

8Department of Chemistry, Stony Brook University, Stony Brook, NY 11974–3400, USA.

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For correspondence: luming@nju.edu.cn xgong@ecust.edu.cn cpg27@cam.ac.uk

Luming Peng

1Key Laboratory of Mesoscopic Chemistry of Ministry of Education, School of Chemistry and Chemical Engineering, Nanjing University, Nanjing 210093, China.

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For correspondence: luming@nju.edu.cn xgong@ecust.edu.cn cpg27@cam.ac.uk

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