Science Advances

Supplementary Materials

This PDF file includes:

  • Synthetic model compounds and compound authentication.
  • Calibration curves and NMR spectra.
  • Fig. S1. 2D HSQC NMR.
  • Fig. S2. Quantitative 13C NMR spectrum of C-LBL.
  • Fig. S3. NBO and thioacidolysis products.
  • Fig. S4. 2D HSQC NMR and molecular weight distributions.
  • Fig. S5. GC-MS total-ion chromatograms of hydrogenolysis monomer products.
  • Fig. S6. Yield and selectivity data.
  • Fig. S7. GPC fractionation of hydrogenolysis products from LBL.
  • Table S1. Compositional analysis of vanilla seed coat CWs.
  • Table S2. Quantitative 13C NMR analysis of C-lignin content in the C-LBL and CW.
  • Table S3. Monomer yields from hydrogenolysis.

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